کد مقاله کد نشریه سال انتشار مقاله انگلیسی نسخه تمام متن
1645961 1517291 2013 4 صفحه PDF دانلود رایگان
عنوان انگلیسی مقاله ISI
Hydrothermal synthesis of flower-like ammonium illite constructed by nanosheets from coal series kaolin
موضوعات مرتبط
مهندسی و علوم پایه مهندسی مواد فناوری نانو (نانو تکنولوژی)
پیش نمایش صفحه اول مقاله
Hydrothermal synthesis of flower-like ammonium illite constructed by nanosheets from coal series kaolin
چکیده انگلیسی

Ammonium illite with hierarchical flower-like structure was synthesized from coal series kaolin under hydrothermal condition at 300 °C for 1 h. The product was characterized by X-ray powder (XRD), Fourier transform infrared spectroscopy (FTIR), scanning electron microscopy (SEM) and transmission electron microscopy (TEM). The results show that the flower-like ammonium illite is constructed by nanosheets with thickness of ca. 20 nm and a diameter of ca. 400 nm. New phase was obtained by calcination of above product at 700 °C for 2 h, and the flower-like morphology was retained after calcination. Furthermore, the specific surface area of ammonium phase powder was calculated to be 197.2 m2/g by BET measurement. The possible formation mechanism for flower-like ammonium illite was proposed and discussed.


► Fist time, nanolayer and flower-like material were synthesized from kaolin.
► The raw material is cheap and easily available in China.
► The process of this method is simple and fast.
► The product has relatively high specific surface area of 197 m2/g.

ناشر
Database: Elsevier - ScienceDirect (ساینس دایرکت)
Journal: Materials Letters - Volume 96, 1 April 2013, Pages 233–236
نویسندگان
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