کد مقاله | کد نشریه | سال انتشار | مقاله انگلیسی | نسخه تمام متن |
---|---|---|---|---|
7616374 | 1494038 | 2016 | 7 صفحه PDF | دانلود رایگان |
عنوان انگلیسی مقاله ISI
Determination of macrocyclic lactones in bovine liver using QuEChERS and HPLC with fluorescence detection
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موضوعات مرتبط
مهندسی و علوم پایه
شیمی
شیمی آنالیزی یا شیمی تجزیه
پیش نمایش صفحه اول مقاله
چکیده انگلیسی
A method for the determination of the macrocyclic lactones Abamectin (ABA), Ivermectin (IVER), Doramectin (DORA) and Moxidectin (MOXI) in liver using HPLC with fluorescence detection is presented. The analytes were extracted and purified using a QuEChERS method. Prior to injection into an HPLC system the sample extracts were reacted with a mixture of 1-methylimidazole, triethylamine, and trifluoroacetic anhydride to obtain the fluorescent derivatives of the analytes. The method has been validated according to EU Decision 2002/657. Recovery for the analytes ranged from 85 to 90%. Repeatibility and Trueness varied between 8-18% and â6 to 6%, respectively and were compliant with the requirements stated in EU Decision 2002/657. Limit of Decision (CCα) were: 22.8 μg kgâ1 (ABA), 126.3 μg kgâ1 (DORA), 118.3 μg kgâ1 (MOXI) and 126.9 μg kgâ1 (IVER).
ناشر
Database: Elsevier - ScienceDirect (ساینس دایرکت)
Journal: Journal of Chromatography B - Volumes 1015â1016, 15 March 2016, Pages 166-172
Journal: Journal of Chromatography B - Volumes 1015â1016, 15 March 2016, Pages 166-172
نویسندگان
David Pimentel-Trapero, Alicia Sonseca-Yepes, Sonia Moreira-Romero, Miguel Hernández-Carrasquilla,