Modeling and experimental study of long term creep damage in austenitic stainless steels

• The damage mechanisms are determined for short and long term creep tests for austenitic stainless steels.
• Riedel model is proposed for predicting the long term creep lifetimes up to about 19 years at 550 °C and 650 °C at low stress for 316LN SSs.
• Riedel model is validated for various other austenitic stainless steels such as 304H, 316H, 321H austenitic stainless steels
• Taking into account the low stress creep rate law, Riedel model allows us to predict lifetimes up to 200,000 h at very high temperature in fair agreement with experimental data.

One of the main challenges for some reactors components in austenitic stainless steels at high temperature in-service conditions is the demonstration of their behavior up to 60 years. The creep lifetimes of these stainless steels require on the one hand to carry out very long term creep tests and on the other hand to understand and to model the damage mechanisms in order to propose physically-based predictions toward 60 years of service. Different batches of austenitic stainless steels like-type 316L with low carbon and closely specified nitrogen content, 316L(N), are subjected to numerous creep tests carried out at various stresses and temperatures between 525 °C and 700 °C up to nearly 50 
•  103 h.Interrupted creep tests show an acceleration of the creep deformation only during the last 15% of creep lifetime, which corresponds to macroscopic necking. The modeling of necking using the Norton viscoplastic power-law allows lifetime predictions in fair agreement with experimental data up to a transition time of about ten thousand hours which is temperature dependent. In fact, one experimental result together with literature ones, shows that the extrapolation of the ‘stress–lifetime’ curves obtained at high stress data leads to large overestimations of lifetimes at low stress. After FEG–SEM observations, these overestimates are mainly due to additional intergranular cavitation as often observed in many metallic materials in the long term creep regime. The modeling of cavity growth by vacancy diffusion along grain boundaries coupled with continuous nucleation proposed by Riedel is carried out. For each specimen, ten FEG–SEM images (about 250 observed grains) are analyzed to determine the rate of cavity nucleation assumed to be constant during each creep test in agreement with many literature results. This measured constant rate is the only measured parameter which is used as input of the Riedel damage model. Lifetimes for long term creep are rather fairly well evaluated by the lowest lifetime predicted by the necking model and the Riedel model predictions. This holds for experimental lifetimes up to 200,000 h and for temperatures between 525 °C and 700 °C. A transition time as well as a transition stress is defined by the intersection of the lifetime curves predicted by the necking and Riedel modelings. This corresponds to the change in damage mechanism. The scatter in lifetimes predicted by the Riedel model induced by the uncertainty of some parameter values is less than a factor of three, similar to experimental scatter. This model is also validated for various other austenitic stainless steels such as 304H, 316H, 321H (creep rupture data provided by NIMS). A transition from power-law to viscous creep deformation regime is reported in the literature at 650 °C–700 °C for steel 316H. Taking into account the low stress creep rate law, it allows us to predict lifetimes up to 200,000 h at very high temperature in fair agreement with experimental data.