کد مقاله | کد نشریه | سال انتشار | مقاله انگلیسی | نسخه تمام متن |
---|---|---|---|---|
7887309 | 1509789 | 2018 | 8 صفحه PDF | دانلود رایگان |
عنوان انگلیسی مقاله ISI
Preparation of TaB2-SiC oxidation protective coating for carbon materials by liquid phase sintering
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کلمات کلیدی
موضوعات مرتبط
مهندسی و علوم پایه
مهندسی مواد
سرامیک و کامپوزیت
پیش نمایش صفحه اول مقاله
چکیده انگلیسی
To control the microstructure and amounts of TaB2 phase in the TaB2-SiC coating, a novel liquid phase sintering method was developed on the basis of in-situ reaction method to prepare the TaB2-SiC coating, which includes synthesis of TaB2 powders and further preparation of TaB2-SiC coating. With Ta2O5, B2O3 and C employed as raw materials, hexagonal TaB2 powders were prepared by carbothermal reduction method at 1500â¯Â°C, whose mean particle size is 491â¯nm. The TaB2, SiC, C powders, and the low melting point phases Si and silica sol were used to prepare the TaB2-SiC coating by liquid phase sintering at 2373â¯K. The thickness of the coating is about 350â¯Âµm. Compared with the SiC coating, the weight loss of the samples modified by TaB2 decreased from 17.7% to 11.8%, and the average weight loss rate of the fastest weightloss zone reduced from â6â¯Ãâ¯10â3 mgâ¯cmâ2 sâ1 to â5â¯Ãâ¯10â3 mgâ¯cmâ2 sâ1. During oxidation, the Ta-oxides would gradually dissolve in the silicate glass to form Ta-Si-O glass ceramics with dendritic structure, which significantly improved the toughness and stability of the glass layer. The Ta-Si-O glass ceramics possesses the ability of sealing and arresting the microcracks, which can enhance the oxidation protective ability of the coating.
ناشر
Database: Elsevier - ScienceDirect (ساینس دایرکت)
Journal: Ceramics International - Volume 44, Issue 9, 15 June 2018, Pages 10708-10715
Journal: Ceramics International - Volume 44, Issue 9, 15 June 2018, Pages 10708-10715
نویسندگان
Xuanru Ren, Lifeng Wang, Peizhong Feng, Ping Zhang, LiTong Guo, Ziyu Li,