کد مقاله کد نشریه سال انتشار مقاله انگلیسی نسخه تمام متن
9603188 43282 2005 5 صفحه PDF دانلود رایگان
عنوان انگلیسی مقاله ISI
Formation characterization of hydroxyapatite on titanium by microarc oxidation and hydrothermal treatment
موضوعات مرتبط
مهندسی و علوم پایه مهندسی شیمی بیو مهندسی (مهندسی زیستی)
پیش نمایش صفحه اول مقاله
Formation characterization of hydroxyapatite on titanium by microarc oxidation and hydrothermal treatment
چکیده انگلیسی
Microarc oxidation (MAO) was performed on titanium in an electrolyte containing calcium glycerphosphate (Ca-GP) and calcium acetate (CA) using a direct current power supply. It was found that the MAO method is suitable forming a ceramic coating containing Ca and P using titanium, and that films display a porous and rough structure on their surface. Samples with a Ca/P ratio of 1.71 were hydrothermally treated in water solution whose pH was adjusted to 7.0-11.0 by adding NaOH at 190°C for 10 h in an autoclave. Hydroxyapatite crystals were precipitated on the film surface after the hydrothermal treatment, and the amount of hydroxyapatite precipitated increased with increasing pH of water solution. The oxide film composition was semiquantitatively analyzed with an electron probe microanalyzer. The microstructures on the sample surfaces were observed by scanning electron microscopy before and after the hydrothermal treatment. The topography of the oxide film was imaged with an atomic force microscope. Its cross section was observed by scanning electron microscopy after being coated with a thin Au film. The surface structures of the films were analyzed by X-ray diffraction.
ناشر
Database: Elsevier - ScienceDirect (ساینس دایرکت)
Journal: Journal of Bioscience and Bioengineering - Volume 100, Issue 1, July 2005, Pages 100-104
نویسندگان
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