کد مقاله کد نشریه سال انتشار مقاله انگلیسی نسخه تمام متن
9743517 1491193 2005 10 صفحه PDF دانلود رایگان
عنوان انگلیسی مقاله ISI
Optimization of the chromatographic conditions for the determination of hormones by gas chromatography with mass spectrometry detection
موضوعات مرتبط
مهندسی و علوم پایه شیمی شیمی آنالیزی یا شیمی تجزیه
پیش نمایش صفحه اول مقاله
Optimization of the chromatographic conditions for the determination of hormones by gas chromatography with mass spectrometry detection
چکیده انگلیسی
A two-factor Doehlert design was subsequently performed to fit a second-order model and jointly optimize the resolution and the peak width through a global desirability function. Thus, the final temperatures of the first and the second ramp are 260 and 300 °C, respectively. The method developed has been validated according to the European Decision 2002/657/EC, including the estimation of the capability of detection (CCβ, X0 = 0, for banned substances) with evaluation of the probability of false positive, α, and of false negative, β.
ناشر
Database: Elsevier - ScienceDirect (ساینس دایرکت)
Journal: Analytica Chimica Acta - Volume 544, Issues 1–2, 15 July 2005, Pages 26-35
نویسندگان
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