کد مقاله | کد نشریه | سال انتشار | مقاله انگلیسی | نسخه تمام متن |
---|---|---|---|---|
9749295 | 1493806 | 2005 | 7 صفحه PDF | دانلود رایگان |
عنوان انگلیسی مقاله ISI
Rapid identification of RoHS-relevant flame retardants from polymer housings by ultrasonic extraction and RP-HPLC/UV
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موضوعات مرتبط
مهندسی و علوم پایه
شیمی
شیمی آنالیزی یا شیمی تجزیه
پیش نمایش صفحه اول مقاله
چکیده انگلیسی
A rapid method was developed for the extraction and identification of RoHS-relevant organic flame retardants in polymer material. Extraction was carried out using ultrasonic supported solvent extraction (USSE) and isopropanol. HPLC separation was achieved using a reversed-phase phenylhexyl-modified column and methanol, containing 2-aminoethanol-buffered, alkaline water. Identification was carried out by scanning UV detection and comparison with a library assembled from spectra of reference substances. The method was used to extract and identify polymer additives in TV and PC monitor housings. The overall runtime required for extraction and chromatographic analysis is less than 10Â min. The limits of detection comply with the recommendations set by the German draft law.
ناشر
Database: Elsevier - ScienceDirect (ساینس دایرکت)
Journal: Journal of Chromatography A - Volume 1066, Issues 1â2, 25 February 2005, Pages 111-117
Journal: Journal of Chromatography A - Volume 1066, Issues 1â2, 25 February 2005, Pages 111-117
نویسندگان
Manfred Pöhlein, Ana Segura Llopis, Marion Wolf, Rudi van Eldik,