کد مقاله کد نشریه سال انتشار مقاله انگلیسی نسخه تمام متن
10547558 964687 2005 12 صفحه PDF دانلود رایگان
عنوان انگلیسی مقاله ISI
Norms and standards for fast pyrolysis liquids
موضوعات مرتبط
مهندسی و علوم پایه شیمی شیمی آنالیزی یا شیمی تجزیه
پیش نمایش صفحه اول مقاله
Norms and standards for fast pyrolysis liquids
چکیده انگلیسی
The main conclusions were: Karl-Fischer titration is recommended for analysing water in pyrolysis liquids. the solids content determined as ethanol insolubles is accurate for white wood (stem wood, no bark or needles) liquids, while a more powerful solvent, like a mixture of methanol and dichloromethane (1:1 vol.%), is required for extractive-rich liquids from feedstocks such as forest residues. for elemental analysis at least triplicates are recommended due to the small sample size. Special attention should be paid to nitrogen standards. They should have a similar range of nitrogen as the sample. Kinematic viscosity is an accurate method at 40 °C for pyrolysis liquids. Rotating viscotesters with a cover at low temperatures (≤50 °C) can also be used. Stability index needs more specific instructions. Results of chemical characterisation were not very consistent. Proper standard solutions have to be used with known amounts of compounds for quantitative analyses.
ناشر
Database: Elsevier - ScienceDirect (ساینس دایرکت)
Journal: Journal of Analytical and Applied Pyrolysis - Volume 73, Issue 2, June 2005, Pages 323-334
نویسندگان
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