کد مقاله کد نشریه سال انتشار مقاله انگلیسی نسخه تمام متن
1170382 960678 2007 6 صفحه PDF دانلود رایگان
عنوان انگلیسی مقاله ISI
Determination of triazine herbicides in sheep liver by microwave-assisted extraction and high performance liquid chromatography
موضوعات مرتبط
مهندسی و علوم پایه شیمی شیمی آنالیزی یا شیمی تجزیه
پیش نمایش صفحه اول مقاله
Determination of triazine herbicides in sheep liver by microwave-assisted extraction and high performance liquid chromatography
چکیده انگلیسی

A multi-residue method developed for the analysis of triazine herbicides, simazine, atrazine, propazine and prometryne, in sheep liver is presented. The method is based on microwave-assisted extraction (MAE) of sheep liver using methanol as extractant and analysis of extracts by high performance liquid chromatography (HPLC) and ultraviolet detection. MAE operational parameters, the solvent type and volume, extraction temperature and time, were optimized in detail with respect to extraction efficiency of the target compounds from sheep liver. The recoveries of the method at two different spiked levels were assessed by analyzing spiked liver samples and were found to be in the range from 90 to 102% with good precision (<11%).

ناشر
Database: Elsevier - ScienceDirect (ساینس دایرکت)
Journal: Analytica Chimica Acta - Volume 590, Issue 1, 2 May 2007, Pages 34–39
نویسندگان
, , , , , , , ,