کد مقاله | کد نشریه | سال انتشار | مقاله انگلیسی | نسخه تمام متن |
---|---|---|---|---|
5141738 | 1495881 | 2017 | 42 صفحه PDF | دانلود رایگان |
عنوان انگلیسی مقاله ISI
Performance evaluation of LC-MS/MS methods for multi-mycotoxin determination in maize and wheat by means of international Proficiency Testing
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کلمات کلیدی
موضوعات مرتبط
مهندسی و علوم پایه
شیمی
شیمی آنالیزی یا شیمی تجزیه
پیش نمایش صفحه اول مقاله
![عکس صفحه اول مقاله: Performance evaluation of LC-MS/MS methods for multi-mycotoxin determination in maize and wheat by means of international Proficiency Testing Performance evaluation of LC-MS/MS methods for multi-mycotoxin determination in maize and wheat by means of international Proficiency Testing](/preview/png/5141738.png)
چکیده انگلیسی
Two Proficiency Testings (PTs) involving eighteen laboratory participants from 10 Countries have been conducted in 2014 for the simultaneous determination of deoxynivalenol, fumonisins B1 and B2, zearalenone, T-2 and HT-2 toxins, ochratoxin A and aflatoxins B1, B2, G1 and G2 in maize and of deoxynivalenol, zearalenone, T-2 and HT-2 toxins and ochratoxin A in wheat, respectively. The aim of PTs was to check next to the laboratory performance the state-of-art of the LC-MS multi-mycotoxin methods used by participants. In addition, the trend of performances of LC-MS methods for multi-mycotoxin determination in maize together with method-related issues was assessed by comparing three PTs organised over the years 2011-2014. Data showed the improvement of laboratory performances with the overall acceptable z-scores that progressively increased from 59% in 2011 PT to 85% in 2014 PT, while the rate of unacceptable z-score decreased from 25% in 2011 PT to 11% in 2014 PT.
ناشر
Database: Elsevier - ScienceDirect (ساینس دایرکت)
Journal: TrAC Trends in Analytical Chemistry - Volume 86, January 2017, Pages 222-234
Journal: TrAC Trends in Analytical Chemistry - Volume 86, January 2017, Pages 222-234
نویسندگان
Annalisa De Girolamo, Biancamaria Ciasca, Joerg Stroka, Stefanka Bratinova, Michelangelo Pascale, Angelo Visconti, Veronica M.T. Lattanzio,