Multiresidue determination of pesticides in industrial and fresh orange juice by hollow fiber microporous membrane liquid-liquid extraction and detection by liquid chromatography-electrospray-tandem mass spectrometry

► A HF-MMLLE for the extraction of a large number of pesticides from juice is proposed. ► A low cost and environmental friendly methodology is presented. ► The method presents linearity, lows LOD/LOQ, good precision, accuracy and robustness.