کد مقاله | کد نشریه | سال انتشار | مقاله انگلیسی | نسخه تمام متن |
---|---|---|---|---|
7787010 | 1500624 | 2015 | 14 صفحه PDF | دانلود رایگان |
عنوان انگلیسی مقاله ISI
Ultrasonic mediated production of carboxymethyl cellulose: Optimization of conditions using response surface methodology
ترجمه فارسی عنوان
تولید اورانیوم کربوکسی متیل سلولز از طریق التراسونیک: بهینه سازی شرایط با استفاده از روش سطح پاسخ
دانلود مقاله + سفارش ترجمه
دانلود مقاله ISI انگلیسی
رایگان برای ایرانیان
کلمات کلیدی
لیترینگ پنبه ای زباله، آلفا سلولز، کاربوکمایتی سلولز، مایکروویو، سونوگرافی، سازگار با محیط زیست،
موضوعات مرتبط
مهندسی و علوم پایه
شیمی
شیمی آلی
چکیده انگلیسی
In the present research the optimization of ultrasound-mediated production of carboxymethyl cellulose under microwave irradiation, towards achieving reduction of chemicals, time of reaction and energy was carried out. Cellulose was extracted and treated by environmentally friendly chlorine free bleaching method using hydrogen peroxide. Produced alpha-cellulose was characterized using Fourier transform infrared spectroscopy (FTIR), scanning electron microscopy (SEM) and thermogravimetric/differential thermal analysis (TG/DTA). Response Surface Methodology (RSM) was used to optimize the preparation of carboxymethyl cellulose (CMC). Highest degree of substitution 0.74 was obtained at 240Â W ultrasonic power for 37Â min followed by etherification at 490W microwave power for 12Â min. Results show that the preparation of CMC from cotton linter using ultrasound and microwave energy can reduce the processing time, chemicals and energy consumption. Additionally, X-ray analysis shows that the ultrasonic energy is able to break cellulose crystals into smaller parts compared to other methods. SEM photographs showed that this treatment is able to remove impurities from raw material.
ناشر
Database: Elsevier - ScienceDirect (ساینس دایرکت)
Journal: Carbohydrate Polymers - Volume 134, 10 December 2015, Pages 278-284
Journal: Carbohydrate Polymers - Volume 134, 10 December 2015, Pages 278-284
نویسندگان
Ahmad Hivechi, S. Hajir Bahrami, Mokhtar Arami, Afzal Karimi,