کد مقاله | کد نشریه | سال انتشار | مقاله انگلیسی | نسخه تمام متن |
---|---|---|---|---|
7791331 | 1500647 | 2014 | 27 صفحه PDF | دانلود رایگان |
عنوان انگلیسی مقاله ISI
Effect of retrogradation time on preparation and characterization of proso millet starch nanoparticles
ترجمه فارسی عنوان
تاثیر زمان رطوبت زایی بر آماده سازی و مشخص نمودن نانوذرات نشاسته پرولینی پروسو
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کلمات کلیدی
نشاسته ارزن پروس، نانوذرات نشاسته، پوسته پوسته شدن مجددا، عقب کشیدن،
موضوعات مرتبط
مهندسی و علوم پایه
شیمی
شیمی آلی
چکیده انگلیسی
Starch nanoparticles were prepared from proso millet starch using a green and facile method combined with enzymolysis and recrystallization. Scanning electron microscopy (SEM), X-ray diffraction (XRD), Fourier transform infrared spectroscopy (FTIR), differential scanning calorimeter (DSC) and thermal gravimetric analysis (TGA) were used to characterize the morphology and crystal structure of the starch nanoparticles prepared with different retrogradation time (0.5, 4, 12, and 24Â h). The results showed that the sizes of the starch nanoparticles were between 20Â nm and 100Â nm. The crystal pattern changed from A-type (native starch) to B-type (nanoparticles), and the relative crystallinity of the nanoparticles increased obviously, as compared with the native starch. The nanoparticles prepared with the 12Â h retrogradation time had the highest degree of crystallinity (47.04%). Compared to conventional acid hydrolysis to make starch nanoparticles, the present approach has the advantage of being quite rapid and presenting a higher yield (about 55%).
ناشر
Database: Elsevier - ScienceDirect (ساینس دایرکت)
Journal: Carbohydrate Polymers - Volume 111, 13 October 2014, Pages 133-138
Journal: Carbohydrate Polymers - Volume 111, 13 October 2014, Pages 133-138
نویسندگان
Qingjie Sun, Min Gong, Ying Li, Liu Xiong,