کد مقاله | کد نشریه | سال انتشار | مقاله انگلیسی | نسخه تمام متن |
---|---|---|---|---|
8954813 | 1646046 | 2019 | 34 صفحه PDF | دانلود رایگان |
عنوان انگلیسی مقاله ISI
Quantitative determination and contamination pattern of perchlorate in tea by ultra performance liquid chromatography and tandem mass spectrometry
ترجمه فارسی عنوان
تعیین کمی و الگوی نفوذ پرکلرات در چای توسط کروماتوگرافی مایع با عملکرد فوق العاده و طیف سنجی جرم دو طرفه
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کلمات کلیدی
Ammonium acetate (PubChem CID: 517165)UPLC-MS/MS - UPLC-MS / MSSolid phase extraction - استخراج فاز جامدAcetonitrile (PubChem CID: 6342) - استونیتریل (PubChem CID: 6342)Acetic acid (PubChem CID: 176) - اسید استیک (PubChem CID: 176)Formic acid (PubChem CID: 284) - اسید فرمیک (PubChem CID: 284)Quantitative determination - تعیین کمیMethanol (PubChem CID: 887) - متانول (PubChem CID: 887)Perchlorate - پرکلراتTEA - چای
موضوعات مرتبط
مهندسی و علوم پایه
شیمی
شیمی آنالیزی یا شیمی تجزیه
چکیده انگلیسی
Perchlorate causes great health concerns for its inhibition on the iodide intake of human. However, the contamination pattern of perchlorate in tea remains unclear although tea is substantially consumed worldwide. Thus, the present study established an efficient method using ultra performance liquid chromatography-tandem mass spectrometry (UPLC-MS/MS) in combination with external standard method, and further lucubrated the contamination level of perchlorate in made tea, fresh tea leaves, along with the waters and soils from tea gardens. Fresh tea leaves with higher maturity generally contains more perchlorate. The observation explains well why the residual of perchlorate in dark tea is generally higher than that in black tea or green tea from the perspective of raw material. In consideration of the ubiquitous existence of perchlorate in waters and soils from tea gardens, perchlorate might accumulate in tea leaves via soil. This study not only provides an alternative quantification method of perchlorate when the isotope internal standard is out of stock, but also illuminates the contamination pattern of perchlorate in tea from planting process.
ناشر
Database: Elsevier - ScienceDirect (ساینس دایرکت)
Journal: Food Chemistry - Volume 274, 15 February 2019, Pages 180-186
Journal: Food Chemistry - Volume 274, 15 February 2019, Pages 180-186
نویسندگان
Yan Liu, Hezhi Sun, Li Zhou, Fengjian Luo, Xinzhong Zhang, Zongmao Chen,