کد مقاله | کد نشریه | سال انتشار | مقاله انگلیسی | نسخه تمام متن |
---|---|---|---|---|
4560312 | 1330499 | 2009 | 5 صفحه PDF | دانلود رایگان |
عنوان انگلیسی مقاله ISI
Determination of ethyl carbamate in cider spirits by HPLC-FLD
دانلود مقاله + سفارش ترجمه
دانلود مقاله ISI انگلیسی
رایگان برای ایرانیان
کلمات کلیدی
موضوعات مرتبط
علوم زیستی و بیوفناوری
علوم کشاورزی و بیولوژیک
دانش تغذیه
پیش نمایش صفحه اول مقاله

چکیده انگلیسی
An analytical method based on HPLC-FLD with prior derivatization with 9-xanthydrol for the determination of ethyl carbamate (EC) in cider spirits is reported. The parameters usually examined in the method validation were evaluated. Good linearity was obtained with a correlation coefficient exceeding 0.9999, the limits of detection and quantitation being 1.64 and 3.56 μg/L, respectively. Recoveries ranged between 94% and 98%, while the precision of the method was <5% (RSD). The method was used to determine EC in samples from different origins with the aim of completing the characterization of cider spirits. Values obtained were usual for this type of drink, ranging between the lower limit of quantitation and 67 μg/L.
ناشر
Database: Elsevier - ScienceDirect (ساینس دایرکت)
Journal: Food Control - Volume 20, Issue 2, February 2009, Pages 139–143
Journal: Food Control - Volume 20, Issue 2, February 2009, Pages 139–143
نویسندگان
Roberto Rodríguez Madrera, Belén Suárez Valles,