کد مقاله کد نشریه سال انتشار مقاله انگلیسی نسخه تمام متن
4560312 1330499 2009 5 صفحه PDF دانلود رایگان
عنوان انگلیسی مقاله ISI
Determination of ethyl carbamate in cider spirits by HPLC-FLD
موضوعات مرتبط
علوم زیستی و بیوفناوری علوم کشاورزی و بیولوژیک دانش تغذیه
پیش نمایش صفحه اول مقاله
Determination of ethyl carbamate in cider spirits by HPLC-FLD
چکیده انگلیسی

An analytical method based on HPLC-FLD with prior derivatization with 9-xanthydrol for the determination of ethyl carbamate (EC) in cider spirits is reported. The parameters usually examined in the method validation were evaluated. Good linearity was obtained with a correlation coefficient exceeding 0.9999, the limits of detection and quantitation being 1.64 and 3.56 μg/L, respectively. Recoveries ranged between 94% and 98%, while the precision of the method was <5% (RSD). The method was used to determine EC in samples from different origins with the aim of completing the characterization of cider spirits. Values obtained were usual for this type of drink, ranging between the lower limit of quantitation and 67 μg/L.

ناشر
Database: Elsevier - ScienceDirect (ساینس دایرکت)
Journal: Food Control - Volume 20, Issue 2, February 2009, Pages 139–143
نویسندگان
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