کد مقاله کد نشریه سال انتشار مقاله انگلیسی نسخه تمام متن
7687732 1495865 2018 45 صفحه PDF دانلود رایگان
عنوان انگلیسی مقاله ISI
Developments and interlaboratory study of the analysis of short-chain chlorinated paraffins
ترجمه فارسی عنوان
تحولات و بررسی بین آزمایشگاهی تجزیه و تحلیل پارافین های کلر زده کوتاه مدت
موضوعات مرتبط
مهندسی و علوم پایه شیمی شیمی آنالیزی یا شیمی تجزیه
چکیده انگلیسی
Participants were requested to analyse test solutions and extracts of various matrices with their method of choice. Thirty-three laboratories participated (9-22 per round), of which 55-81% were able to submit data. Large differences in results between laboratories were found (CVs 23-137%) but results improved over time, while the levels in the test materials decreased. In the last round acceptable CV values (<25%) were obtained for the test solution. In the last round, results obtained by the GC-ECNI-LRMS technique varied most, which is disconcerting as this technique is most commonly applied. We strongly suggest to continue monitoring comparability of laboratories to assess consensus in SCCP analysis, with a focus on quantification procedures applied.
ناشر
Database: Elsevier - ScienceDirect (ساینس دایرکت)
Journal: TrAC Trends in Analytical Chemistry - Volume 102, May 2018, Pages 32-40
نویسندگان
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