کد مقاله | کد نشریه | سال انتشار | مقاله انگلیسی | نسخه تمام متن |
---|---|---|---|---|
7687732 | 1495865 | 2018 | 45 صفحه PDF | دانلود رایگان |
عنوان انگلیسی مقاله ISI
Developments and interlaboratory study of the analysis of short-chain chlorinated paraffins
ترجمه فارسی عنوان
تحولات و بررسی بین آزمایشگاهی تجزیه و تحلیل پارافین های کلر زده کوتاه مدت
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کلمات کلیدی
موضوعات مرتبط
مهندسی و علوم پایه
شیمی
شیمی آنالیزی یا شیمی تجزیه
چکیده انگلیسی
Participants were requested to analyse test solutions and extracts of various matrices with their method of choice. Thirty-three laboratories participated (9-22 per round), of which 55-81% were able to submit data. Large differences in results between laboratories were found (CVs 23-137%) but results improved over time, while the levels in the test materials decreased. In the last round acceptable CV values (<25%) were obtained for the test solution. In the last round, results obtained by the GC-ECNI-LRMS technique varied most, which is disconcerting as this technique is most commonly applied. We strongly suggest to continue monitoring comparability of laboratories to assess consensus in SCCP analysis, with a focus on quantification procedures applied.
ناشر
Database: Elsevier - ScienceDirect (ساینس دایرکت)
Journal: TrAC Trends in Analytical Chemistry - Volume 102, May 2018, Pages 32-40
Journal: TrAC Trends in Analytical Chemistry - Volume 102, May 2018, Pages 32-40
نویسندگان
L.M. van Mourik, I. van der Veen, S. Crum, J. de Boer,