کد مقاله | کد نشریه | سال انتشار | مقاله انگلیسی | نسخه تمام متن |
---|---|---|---|---|
9743721 | 1491198 | 2005 | 6 صفحه PDF | دانلود رایگان |
عنوان انگلیسی مقاله ISI
Determination of carotene, tocopherols and tocotrienols in residue oil from palm pressed fiber using pressurized liquid extraction-normal phase liquid chromatography
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کلمات کلیدی
موضوعات مرتبط
مهندسی و علوم پایه
شیمی
شیمی آنالیزی یا شیمی تجزیه
پیش نمایش صفحه اول مقاله
![عکس صفحه اول مقاله: Determination of carotene, tocopherols and tocotrienols in residue oil from palm pressed fiber using pressurized liquid extraction-normal phase liquid chromatography Determination of carotene, tocopherols and tocotrienols in residue oil from palm pressed fiber using pressurized liquid extraction-normal phase liquid chromatography](/preview/png/9743721.png)
چکیده انگلیسی
Pressurized liquid extraction (PLE) along with normal phase liquid chromatography (NPLC) is evaluated as a new approach for the determination of β-carotene and Vitamin E isomers in residue oil obtained from palm pressed fiber (PPF). The relative extraction recoveries obtained by optimized PLE were found to be equivalent (â¼100%) to conventional Soxhlet extraction. Optimized PLE was obtained (5 g of sample, 80 °C, 1500 psi, 2à 10 min static extractions with flush volume 50%) combined with NPLC system. Typical extractions give 3.7-4.0 mg mlâ1 of Vitamin E isomers and β-carotene of 3.3-3.5 mg mlâ1, which is similar to or greater than classical Soxhlet extraction with n-hexane or chloroform. The new developed method demonstrated an acceptable performance with good efficiency in terms of total extraction time, total solvent usage, total β-carotene and Vitamin E isomers contents as well as exceptional method repeatability.
ناشر
Database: Elsevier - ScienceDirect (ساینس دایرکت)
Journal: Analytica Chimica Acta - Volume 538, Issues 1â2, 4 May 2005, Pages 71-76
Journal: Analytica Chimica Acta - Volume 538, Issues 1â2, 4 May 2005, Pages 71-76
نویسندگان
M. Marsin Sanagi, H.H. See, Wan Aini Wan Ibrahim, Ahmedy Abu Naim,