کد مقاله | کد نشریه | سال انتشار | مقاله انگلیسی | نسخه تمام متن |
---|---|---|---|---|
1204501 | 965155 | 2009 | 4 صفحه PDF | دانلود رایگان |
عنوان انگلیسی مقاله ISI
Biogenic amine determination in wines using solid-phase extraction: A comparative study
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کلمات کلیدی
موضوعات مرتبط
مهندسی و علوم پایه
شیمی
شیمی آنالیزی یا شیمی تجزیه
پیش نمایش صفحه اول مقاله
چکیده انگلیسی
Biogenic amines in wine usually are analyzed by high-performance liquid chromatography after direct derivatization. A method of isolation based on solid-phase extraction (SPE) with mixed-mode resins (Oasis MCX, reverse-phase and ion exchange) was developed. The different stages of the isolation process (loading, elution and washing) were optimized to obtain a simple procedure that yields a clean chromatogram. The relative standard deviation (%RSD) of the retention times and relative areas was less than 0.3% and 6%, respectively. Limits of quantification were lower than 0.16 mg L−1 for all the amines and the linear range of concentration was 0.16–8 mg L−1 for putrescine, cadaverine and tyramine, and up to 10 mg L−1 for histamine.
ناشر
Database: Elsevier - ScienceDirect (ساینس دایرکت)
Journal: Journal of Chromatography A - Volume 1216, Issue 15, 10 April 2009, Pages 3398–3401
Journal: Journal of Chromatography A - Volume 1216, Issue 15, 10 April 2009, Pages 3398–3401
نویسندگان
A. Peña-Gallego, P. Hernández-Orte, J. Cacho, V. Ferreira,