کد مقاله | کد نشریه | سال انتشار | مقاله انگلیسی | نسخه تمام متن |
---|---|---|---|---|
1673199 | 1008945 | 2009 | 4 صفحه PDF | دانلود رایگان |
عنوان انگلیسی مقاله ISI
Mechanical properties of hybrid sol-gel derived films as a function of composition and thermal treatment
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کلمات کلیدی
موضوعات مرتبط
مهندسی و علوم پایه
مهندسی مواد
فناوری نانو (نانو تکنولوژی)
پیش نمایش صفحه اول مقاله

چکیده انگلیسی
Sol-gel coatings derived from glycidoxypropyltrimethoxysilane (GLYMO) and/or methyltrimethoxysilane (MTMS) and silica nanoparticle filler were prepared. The mechanical properties of the coatings were measured as a function of coating composition and thermal treatment temperature using nanoindentation. Thermogravimetric analysis was used to determine the material loss rate during heating and the thermal stability of the materials. The coating hardness (H) and reduced modulus (Er) strongly increased with increasing thermal treatment temperatures. The changes in the mechanical properties were found to correlate with the conversion of silanol groups measured by infrared spectroscopy. The partial replacement of MTMS by GLYMO in the coatings initially increased the hardness and modulus but larger proportions of GLYMO reduced H and Er. It was found that both thermal treatment temperature and variation in coating composition could result in large changes in the key material ratio of H3/Er2, that in turn could strongly influence the mechanical response of the coating.
ناشر
Database: Elsevier - ScienceDirect (ساینس دایرکت)
Journal: Thin Solid Films - Volume 517, Issue 17, 1 July 2009, Pages 4888-4891
Journal: Thin Solid Films - Volume 517, Issue 17, 1 July 2009, Pages 4888-4891
نویسندگان
S. Nemeth, Y.C. Liu,