کد مقاله | کد نشریه | سال انتشار | مقاله انگلیسی | نسخه تمام متن |
---|---|---|---|---|
9813074 | 1518125 | 2005 | 8 صفحه PDF | دانلود رایگان |
عنوان انگلیسی مقاله ISI
Morphology control and texture of Fe3O4 nanoparticle-coated polystyrene microspheres by ethylene glycol in forced hydrolysis reaction
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کلمات کلیدی
موضوعات مرتبط
مهندسی و علوم پایه
مهندسی مواد
فناوری نانو (نانو تکنولوژی)
پیش نمایش صفحه اول مقاله
چکیده انگلیسی
The effects of ethylene glycol (EG) on morphology and texture of the magnetite shell/core polystyrene microspheres produced from a forced hydrolysis reaction of FeCl2 solution were investigated. The morphology of magnetite-shell of synthetic composite spheres was dependent on EG concentration. They changed from large sphere with the shell-thickness of ca. 35 nm to corrugated films with increasing EG concentration in the coating solution accompanying a reduction of their shell-particles size to 10 nm. The magnetite coating on latex is formed by a phase transformation from β-FeOOH to magnetite due to the oxidation from Fe2+ to Fe3+ and adsorption of a lot of Fe2+ ions. The shell magnetite formed with EG was hydro-magnetite with a crystal lattice distortion, and they exhibited a polycrystalline nature. The nanoporous magnetite shell was produced in the presence of EG acting as a templating agent. This paper indicates that good superparamagnetic magnetite particles in shell have been synthesized at 5% EG concentration.
ناشر
Database: Elsevier - ScienceDirect (ساینس دایرکت)
Journal: Thin Solid Films - Volume 471, Issues 1â2, 3 January 2005, Pages 105-112
Journal: Thin Solid Films - Volume 471, Issues 1â2, 3 January 2005, Pages 105-112
نویسندگان
Zhongbing Huang, Fangqiong Tang, Lin Zhang,